2,4,6-Trimethyl-1,3-phenylenediamine(3102-70-3) MS

Product Name2,4,6-Trimethyl-1,3-phenylenediamine

CAS 3102-70-3

Molecular FormulaC9H14N2

Molecular Weight150.22

InChIInChI=1S/C9H14N2/c1-5-4-6(2)9(11)7(3)8(5)10/h4H,10-11H2,1-3H3

InChIKey ZVDSMYGTJDFNHN-UHFFFAOYSA-N

SmilesC1(N)=C(C)C=C(C)C(N)=C1C

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2,4,6-Trimethyl-1,3-phenylenediamine(3102-70-3) MS
Mass

MS-NW-7894          
2,4,6-trimethyl-m-phenylenediamine
C9H14N2             (Mass of molecular ion:    150)

   Source Temperature: 150 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      18.0       1.8
      27.0       1.6
      28.0       3.8
      30.0       1.3
      39.0       3.7
      41.0       2.2
      42.0       3.0
      51.0       1.8
      52.0       2.2
      53.0       2.5
      54.0       3.0
      61.0       3.4
      63.0       1.1
      65.0       3.5
      66.0       2.7
      67.0       4.9
      67.5       1.3
      73.0       1.4
      74.0       4.4
      74.5       1.0
      75.0       7.6
      77.0       4.1
      78.0       1.3
      79.0       2.6
      80.0       1.4
      91.0       3.2
      92.0       1.1
      93.0       2.1
      94.0       2.4
      95.0       1.0
     103.0       1.6
     104.0       1.2
     105.0       3.2
     106.0       5.1
     107.0       5.9
     108.0       3.5
     109.0       1.8
     110.0       1.0
     117.0       3.4
     118.0       5.9
     119.0       1.3
     120.0       3.0
     121.0       2.0
     122.0       7.3
     123.0       1.1
     130.0       1.8
     131.0       1.2
     132.0       8.8
     133.0       8.3
     134.0       5.7
     135.0      37.2
     136.0       3.6
     147.0       1.2
     148.0       1.7
     149.0      63.3
     150.0     100.0
     151.0      10.6

90 MHz in DMSO-d6

2,4,6-Trimethyl-1,3-phenylenediamine(3102-70-3) MS

¹H NMR	89.56 MHz
C₉ H₁₄ N₂	0.055 g : 0.5 ml DMSO-d₆
2,4,6-trimethyl-m-phenylenediamine

    Assign.     Shift(ppm)

      A             6.43
      B             4.06
      C             1.94
      D             1.866

     Hz     ppm     Int.

    575.63   6.428    116
    363.63   4.061    112
    182.00   2.033     23
    181.31   2.025     24
    173.94   1.943   1000
    167.25   1.868    577

in CDCl3