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ChemicalBook > Product Catalog >Chemical Reagents >Organic reagents >fatty acid >2,6-Dichlorophenylacetic acid

2,6-Dichlorophenylacetic acid

2,6-Dichlorophenylacetic acid Suppliers list
Company Name: Hebei Chuanghai Biotechnology Co,.LTD
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Products Intro: Product Name:2,6-Dichlorophenylacetic acid
CAS:6575-24-2
Purity:99.9 Package:1KG;9.00;USD
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Products Intro: Product Name:2,6-Dichlorophenylacetic acid
CAS:6575-24-2
Purity:99% Package:1KG;0.00;USD|25KG;0.00;USD|1000KG;0.00;USD
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CAS:6575-24-2
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Products Intro: Product Name:2,6-dichlorophenylacetic acid
CAS:6575-24-2
Purity:98%(min,HPLC) Package:1G;1KG;100KG
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Products Intro: Product Name:2,6-Dichlorophenylacetic acid
CAS:6575-24-2
Purity:99% Package:25KG;USD

2,6-Dichlorophenylacetic acid manufacturers

2,6-Dichlorophenylacetic acid Basic information
Product Name:2,6-Dichlorophenylacetic acid
Synonyms:TIMTEC-BB SBB003503;Benzeneacetic acid, 2,6-dichloro-;2,6-Dichlorophenyl acetic acid 98%;2,6-Dichlorophenylacetic acid, 98+%;Acetic acid, (2,6-dichlorophenyl)-;2,6-Dichlorophenylacetic acid,99%;6-Dichlorophenylacetic acid;2,6-two chlorophenyl acetic acid
CAS:6575-24-2
MF:C8H6Cl2O2
MW:205.04
EINECS:229-504-0
Product Categories:C8;Carbonyl Compounds;Carboxylic Acids;Aromatic Phenylacetic Acids and Derivatives;Phenylacetic acid;Acids and Derivatives
Mol File:6575-24-2.mol
2,6-Dichlorophenylacetic acid Structure
2,6-Dichlorophenylacetic acid Chemical Properties
Melting point 158-161 °C (lit.)
Boiling point 294.45°C (rough estimate)
density 1.3806 (rough estimate)
refractive index 1.5490 (estimate)
storage temp. Sealed in dry,Room Temperature
solubility DMSO (Slightly), Methanol (Slightly)
form Solid
pka3.80±0.10(Predicted)
color White to Off-White
BRN 1952744
InChIInChI=1S/C8H6Cl2O2/c9-6-2-1-3-7(10)5(6)4-8(11)12/h1-3H,4H2,(H,11,12)
InChIKeySFAILOOQFZNOAU-UHFFFAOYSA-N
SMILESC1(CC(O)=O)=C(Cl)C=CC=C1Cl
CAS DataBase Reference6575-24-2(CAS DataBase Reference)
NIST Chemistry Reference2,6-Dichlorophenylacetic acid(6575-24-2)
EPA Substance Registry SystemBenzeneacetic acid, 2,6-dichloro- (6575-24-2)
Safety Information
Hazard Codes Xi
Risk Statements 36/37/38
Safety Statements 37/39-26-26/37/39-36
WGK Germany 3
Hazard Note Irritant
HS Code 29163900
MSDS Information
ProviderLanguage
2,6-Dichlorophenylacetic acid English
ACROS English
ALFA English
2,6-Dichlorophenylacetic acid Usage And Synthesis
Chemical Propertieswhite crystalline powder
Uses2,6-Dichlorophenylacetic acid is an inhibitor of isopenicillin N synthase (IPNS) and acyl-CoA: 6-APA acyltransferase. 2,6-Dichlorophenylacetic acid is also part of a group of phenylacetate derivatives that have cytostatic activity against tumour cells.
PreparationThe preparation of the 2, 6-dichlorophenylacetic acid:
the method comprises the following steps: 2, 6-dichlorotoluene is used as a raw material, and is catalyzed by a complex catalyst formed by transition metal and a ligand (wherein, a transition metal catalyst precursor is preferably palladium chloride, an oxidant is preferably TBP (tert-butyl peroxy ether), and a ligand is preferably Xantphos (4, 5-bis (diphenylphosphino) -9, 9-dimethyl xanthene)) in the presence of an alcohol and a catalyst and an oxidant to obtain 2, 6-dichlorophenylacetic acid, and the ethyl 2, 6-dichlorophenylacetate is prepared by hydrolysis and acidification, wherein the total yield is 68.4%. See patent document US2013303798, the reaction procedure is described as synthetic route 1.
preparation of the 2, 6-dichlorophenylacetic acid
In the above synthetic route 1, the preparation process of the intermediate ethyl 2, 6-dichlorophenylacetate requires the use of carbon monoxide for high-temperature and high-pressure reaction, and has poor operation safety, high equipment requirement, high cost, and is not favorable for cost reduction and green production of 2, 6-dichlorophenylacetic acid.
Purification MethodsCrystallise the acid from aqueous EtOH. [Beilstein 9 III 2272.]
Tag:2,6-Dichlorophenylacetic acid(6575-24-2) Related Product Information
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