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Product Name:(N-METHYL-N-PHENYLAMINO)TRIPHENYLPHOSPHONIUM IODIDE
CAS:34257-63-1
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Product Name:(N-Methyl-N-phenylaMino)triphenylphosphoniuM Iodide
CAS:34257-63-1
Purity:98.0%(T) Package:10G
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Meryer (Shanghai) Chemical Technology Co., Ltd.
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Product Name:(N-Methyl-N-phenylaMino)triphenylphosphoniuM Iodide
CAS:34257-63-1
Purity:98% Package:10g Remarks:M1151
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(N-METHYL-N-PHENYLAMINO)TRIPHENYLPHOSPHONIUM IODIDE manufacturers
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| | (N-METHYL-N-PHENYLAMINO)TRIPHENYLPHOSPHONIUM IODIDE Basic information |
| Product Name: | (N-METHYL-N-PHENYLAMINO)TRIPHENYLPHOSPHONIUM IODIDE | | Synonyms: | N-METHYLANILINOTRIPHENYLPHOSPHONIUM IODIDE;(N-METHYL-N-PHENYLAMINO)TRIPHENYLPHOSPHONIUM IODIDE;(N-METHYLPHENYLAMINO)TRIPHENYL- &;Phosphorus(1+), (N-methylbenzenaminato)triphenyl-, iodide, (T-4)-;murahashi's reagent;(N-Methylphenylamino)T;(N-METHYL-N-PHENYLAMINO)-TRIPHENYLPHOSPH;(N-Methylphenylamino)triphenylphosphonium iodide | | CAS: | 34257-63-1 | | MF: | C25H23INP | | MW: | 495.34 | | EINECS: | | | Product Categories: | Phosphonium Compounds | | Mol File: | 34257-63-1.mol |  |
| | (N-METHYL-N-PHENYLAMINO)TRIPHENYLPHOSPHONIUM IODIDE Chemical Properties |
| Melting point | 238-239°C | | solubility | sol DMF, EtOAc. Behaves as a Wittig-type reagent in terms of solubility. | | form | powder to crystal | | color | White to Yellow to Orange | | CAS DataBase Reference | 34257-63-1(CAS DataBase Reference) |
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| | (N-METHYL-N-PHENYLAMINO)TRIPHENYLPHOSPHONIUM IODIDE Usage And Synthesis |
| Uses | (N-Methyl-N-phenylamino)triphenylphosphonium Iodide is used to synthesis of amines from alcohols; synthesis of unsymmetrical sulfides; synthesis of alkenes from allyl
alcohols; synthesis of 1,3-dienes. | | Preparation | Preparative Method of (N-Methyl-N-phenylamino)triphenylphosphonium Iodide: phenyliminotriphenylphosphorane is reacted with excess Iodomethane at reflux for 2
h. Removal of MeI followed by recrystallization gives a quantitative yield.[1] | | storage | (N-Methyl-N-phenylamino)triphenylphosphonium Iodide stores in sealed bottle on bench. Do not breathe dust, fumes, or vapor.
Avoid contact with skin and eyes. Use in a fume hood. | | References | 1. Tanigawa, Y.; Kanamaru, H.; Sonoda, A.; Murahashi, S-I. JACS 1977, 99, 2361. |
| | (N-METHYL-N-PHENYLAMINO)TRIPHENYLPHOSPHONIUM IODIDE Preparation Products And Raw materials |
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