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ChemicalBook CAS DataBase List methyl 2-(4-nitrophenyl)propionate
50415-69-5

methyl 2-(4-nitrophenyl)propionate synthesis

12synthesis methods
-

Yield:50415-69-5 100%

Reaction Conditions:

with sulfuric acid at 20;

Steps:

24 (+-)-2-[4-[3-(hexylcarbamoyloxy)phenyl]-3-hydroxy-phenyl]propanoic acid (29d)

4.1.24
(+-)-Methyl 2-(4-nitrophenyl)propanoate (24e)
To a solution of 23e (1.95 g, 10 mmol) in MeOH (20 mL), concentrated H2SO4 (0.1 mL) was added and the resulting solution was stirred overnight at rt.
After solvent evaporation, the crude oil was diluted with Et2O (15 mL) and filtered through a pad of SiO2 to afford 24e as yellow oil (2.10 g, quant.)

References:

Migliore, Marco;Habrant, Damien;Sasso, Oscar;Albani, Clara;Bertozzi, Sine Mandrup;Armirotti, Andrea;Piomelli, Daniele;Scarpelli, Rita [European Journal of Medicinal Chemistry,2016,vol. 109,p. 216 - 237]

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