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N-??????????
N-?????????? ??? ???
?? ??:
1116-54-7
???:
N-??????????
???(??):
N-??????????;N-??????????(N-NITROSODIETHANOLAMINE);2,2'-(????????)?????
???:
N-NITROSODIETHANOLAMINE
???(??):
ndela;nci-c55583;rcrawastenumberu173;diaethanolnitrosamin;DIETHANOLNITROSAMINE;diethanolnitrosoamine;nitrosodiethanolamine;nitrosoiminodiethanol;N-DIETHANOLNITROSAMINE;N-Nitrosoamindiethanol
CBNumber:
CB8401443
???:
C4H10N2O3
??? ??:
134.13
MOL ??:
1116-54-7.mol
MSDS ??:
SDS

N-?????????? ??

???
200 °C (decomp)
?? ?
bp0.01 125°
??
1,26 g/cm3
???
nD20 1.4849
???
11℃
?? ??
2-8°C
???
Completely miscible in water
???
DMSO (Soluble), Ethyl Acetate (Sparingly), Methanol (Soluble), Water (Sparingly)
??? ??
clear liquid to slightly cloudy liquid
?? ?? (pKa)
13.76±0.10(Predicted)
??
?? ????? ????
Merck
14,6634
BRN
1762620
CAS ??????
1116-54-7(CAS DataBase Reference)
IARC
2B (Vol. 17, Sup 7, 77) 2000
EPA
N-Nitrosodiethanolamine (1116-54-7)
??
  • ?? ? ?? ??
  • ?? ? ???? ?? (GHS)
??? ?? T,F
?? ???? ?? 45-11
????? 53-45-16
????(UN No.) UN 1993 3/PG 2
WGK ?? 1
RTECS ?? KL9550000
HS ?? 2922.19.9690
?? ?? 3.1
???? II
?? ?? ??? 1116-54-7(Hazardous Substances Data)
?? LD50 orl-rat: 7500 mg/kg GISAAA 40(1),81,75
????(GHS): GHS hazard pictogramsGHS hazard pictogramsGHS hazard pictograms
?? ?: Danger
??·?? ??:
?? ??·?? ?? ?? ?? ?? ?? ? ?? ?? P- ??
H225 ???? ?? ? ?? ??? ?? ?? 2 ?? GHS hazard pictograms P210,P233, P240, P241, P242, P243,P280, P303+ P361+P353, P370+P378,P403+P235, P501
H319 ?? ?? ??? ??? ?? ? ?? ?? ??? ?? ?? 2A ?? GHS hazard pictograms P264, P280, P305+P351+P338,P337+P313P
H350 ?? ??? ? ?? (????? ?? ???? ???? ???? ??? ?? ????? ??? ???? ??) ??? ?? ?? 1A, 1B ?? GHS hazard pictograms
??????:
P201 ?? ? ?? ???? ?????.
P210 ?·???·??·????? ????? - ?? ???.
P305+P351+P338 ?? ??? ? ?? ?? ???? ????. ???? ?????? ?????. ?? ????.
P308+P313 ?? ?? ??? ???? ???? ??· ??? ????.
NFPA 704
3
2 0

N-?????????? C??? ??, ??, ??

??? ??

Reddish Yellow Oil

??

A potent liver carcinogen in several species of animals, is one of the most widespread N-nitroso compounds in the human environment.

?? ??

Yellow to dark brown very viscous liquid with no distinct odor.

??? ?? ??

Water soluble.

?? ???

N-NITROSODIETHANOLAMINE can react with alkoxides. N-NITROSODIETHANOLAMINE reacts with sulfuric acid at temperatures above 311° F.

????

ACUTE/CHRONIC HAZARDS: N-NITROSODIETHANOLAMINE may be harmful by eye or skin contact, inhalation or ingestion. It is an irritant and, when heated to decomposition, it emits toxic fumes of carbon monoxide, carbon dioxide and nitrogen oxides.

????

Flash point data for N-NITROSODIETHANOLAMINE are not available; however, N-NITROSODIETHANOLAMINE is probably combustible.

Safety Profile

Confirmed carcinogen with experimental carcinogenic, neoplastigenic, and tumorigenic data.Mildly toxic by ingestion. Mutation data reported. When heated to decomposition it emits toxic fumes of NOx. See also N-NITROSO COMPOUNDS and ALCOHOLS.

Carcinogenicity

N-Nitrosodiethanolamine is reasonably anticipated to be a human carcinogen based on sufficient evidence of carcinogenicity from studies in experimental animals.

Purification Methods

Purify NDELA by dissolving the amine (0.5g) in 1-propanol (10mL) and 5g of anhydrous Na2SO4 added with stirring. After standing for 1-2hours, it is filtered and passed through a chromatographic column packed with 10mL of AG 50W x 8 (H+form 50-100mesh, a strongly acidic cation exchanger). The eluent and washings (50 mL EtOH) are combined and evaporated to dryness at 35o. It has also been extracted with EtOH from the nitrosation mixture of ethanolamine, filtered and distilled under high vacuum. [Fukuda et al. Anal Chem 53 2000 1981, Jones & Wilson J Chem Soc 550, 1949, Beilstein 1 III 721, see Spiegelhalder et al. N-Nitroso Compounds: Occurrence Biological Effects and Relevance in Human Cancer (eds. O’Neill et al. IARC Scientific Publications No 57; IARC Lyon p943 1984.] Possible

N-?????????? ?? ?? ? ???

???

Ethanol, 2-[(3,7-dimethyloctyl)nitrosoamino]- Ethanol, 2,2'-[(3,7-dimethyl-2,6-octadienyl)imino]bis-, (E)- (9CI) (E)-2-((3,7-???-2,6-?????)???????)??? S-????-N-??????? S-????????? ??????? ???????

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???( 114)?? ??
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