ChemicalBook >?? ???? >??? ??>????? ???>?? ???? ? ???>H-DL-ASP(OME)-OME HCL

H-DL-ASP(OME)-OME HCL

H-DL-ASP(OME)-OME HCL ??? ???

?? ??:: 14358-33-9

???:: H-DL-ASP(OME)-OME HCL

???(??):: DL-Asp(OMe)-OMe·HCl;H-DL-ASP(OME)-OME HCL;Asciminib Impurity 16;DL-ASPARTIC ACID(OME)-OME HCL;dl-asparticaciddimethylesterHCl;H-DL-ASP(OME)-OME HCL USP/EP/BP;dimethyl 2-aminosuccinate hydrochloride;(1,4-dimethoxy-1,4-dioxobutan-2-yl)azanium;DL-ASPARTIC ACID DIMETHYL ESTER HYDROCHLORIDE;1,4-dimethyl 2-aminobutanedioate hydrochloride

CBNumber:: CB6309178

???:: C6H12ClNO4

??? ??:: 197.62

MOL ??:: 14358-33-9.mol

?? ?? 81

H-DL-ASP(OME)-OME HCL ??

???: 115-116.5℃ (ethanol ethyl acetate )

?? ??: Inert atmosphere,2-8°C

???: Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.

??? ??: ??

??: White to off-white

?? ? ?? ??
?? ? ???? ?? (GHS)

??? ??	Xi
?? ???? ??	42/43
?????	36/37

????(GHS):

?? ?:

Warning

??·?? ??:

??	??·?? ??	?? ??	??	?? ?	?? ??	P- ??
H317	????? ?? ??? ??? ? ??	?? ??? ??	?? 1	??		P261, P272, P280, P302+P352,P333+P313, P321, P363, P501

??????:

P261	??·?·??·???·??·...·????? ??? ????.
P272	??? ??? ??? ??? ???? ???.
P280	????/???/???/?????? ?????.
P302+P352	??? ??? ??? ?? ????.
P321	(…) ??? ???.
P333+P313	????? ?? ??? ???? ???? ??·??? ????.
P363	?? ??? ??? ??? ?????.
P501	...? ??? / ??? ?? ???.

H-DL-ASP(OME)-OME HCL C??? ??, ??, ??

??? ??

White or off-white crystal

Purification Methods

Crystallise it from absolute MeOH. [Kovach et al. J Am Chem Soc 107 7360 1985.] The diethyl ester has pK25 6.4.

H-DL-ASP(OME)-OME HCL ?? ?? ? ???

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H-DL-ASP(OME)-OME HCL ?? ??

???( 81)?? ??

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H-DL-ASP(OME)-OME HCL ?? ??:

H-ASP(OET)-OET HCL D-ASPARTIC ACID DIMETHYL ESTER HYDROCHLORIDE Dimethyl L-aspartate hydrochloride H-ASP(OTBU)-OTBU HCL DL-Aspartic acid ASPARTIC ACID(OTBU)-ALLYL ESTER HCL H-ASP(OBZL)-OBZL HCL H-ASP(OME)-OTBU HCL H-DL-ASP(OME)-OME HCL H-ASP(OBZL)-OTBU HCL N-ALPHA-CARBOBENZOXY-L-ASPARTIC ACID BETA-T-BUTYL ESTER-ALPHA-BENZYL ESTER HYDROCHLORIDE H-D-Asp(OtBu)-OtBu · HCl FMOC-ASP(OTBU)-2-CHLOROTRITYL RESIN H-D-ASP(OTBU)-ALLYL ESTER HCL H-ASP(OTBU)-OME HCL H-DL-ASP-OME H-L-MEASP(TBU)-OME HCL METHYL 4-BENZYL-6-(3-CHLORO-4-METHOXYPHENYL)-1,3-DIOXOHEXAHYDRO-1H-FURO[3,4-C]PYRROLE-4-CARBOXYLATE

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