?? ?? 102?
|
|
?? ?? 102? ??
- ???
- >300oC
- ??
- 1.772[at 20℃]
- ???
- 0Pa at 25℃
- ?? ??
- Inert atmosphere,Room Temperature
- ???
- DMSO (Slightly, Heated, Sonicated), Methanol (Slightly, Heated), Water (Slightly)
- ?? ?? ??
- 16255
- ??? ??
- ??
- ??
- ????? ?????
- ???
- 305.21g/L at 20℃
- ?? ??(λmax)
- 350 nm (2nd)
506 nm
- BRN
- 4122340
- ???
- ???
- InChIKey
- MSUZYPTYNUUBFH-ZPZFBZIMSA-N
- SMILES
- N(/C1=C(C=CC2=CC(S(O)(=O)=O)=CC(S(O)(=O)=O)=C12)O)=N\C1=CC=C(S(O)(=O)=O)C2=CC=CC=C12.[NaH]
- LogP
- -2.267 at 20℃
- ?? ? ?? ??
- ?? ? ???? ?? (GHS)
| ????? | 22-24/25 | ||
|---|---|---|---|
| WGK ?? | 2 | ||
| RTECS ?? | QJ6530000 | ||
| HS ?? | 32041200 | ||
| ?? ?? ??? | 2611-82-7(Hazardous Substances Data) | ||
| ?? | LD50 oral in rat: > 8gm/kg | ||
| ???? ?? | KE-06701 |
| ????(GHS): |
|
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|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| ?? ?: | Warning | |||||||||||||||||||||||||||||||||||
| ??·?? ??: |
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| ??????: |
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?? ?? 102? C??? ??, ??, ??
????
? (1) ???? : ????? ? ??????? ? ?, ? ?? 0.2% ????? ??.
??(2) ??? ? ??? : ????? ? ??? ? ?????? ? ?, ? ??? 8.0% ????? ??.
??(3) ?? : ? ??? ?????? ?? ??? ?, ? ?? 4.0ppm ????? ??.
??(4) ? : ? ?? 5.0g? ??? ??????? ?? ?????????????? ?? ??? ?, ? ?? 2.0ppm ????? ??.
??(5) ??? : ? ?? 5.0g? ??? ??????? ?? ?????????????? ?? ??? ?, ? ?? 1.0ppm ????? ??.
??(6) ?? : ? ??? ?????? ?? ??? ?, ? ?? 1.0ppm ????? ??.
??(7) ??? ?? : 「???????3?」 ????(9)? ?? ????.
??(8) ????? ? ????? : ? ?? 100mg? ?? ???????(1.54→1,000)? ??? ?? ??? 100mL? ? ?? ?????? ??. ??? ?????????? 24?? ??? 4-???-1-????????????????, 7-????-1,3-????????????, 3-????-2,7-????????????, 6-????-2-??????????? ? 7-????-1,3,6-????????????? 10.0mg? ?? ??? ???????(1.54→1,000)? ??? ?? 100mL? ? ?? ?????? ?? ????? ????? ? ?????? ??, ???? ???? ?? 4-???-1-???????????(4-amino-1-naphtahlenesulfonic acid monosodium salt), 7-????-1,3-????????????(7-hydroxy-1,3- naphthalene disulfonic acid disodium salt), 3-????-2,7-????????????(3-hydroxy-2,7-naphthalenedisulfonic acid disodium salt), 6-????-2-???????????(6-hydroxy-2- naphthalenesulfonic acid monosodium salt) ? 7-????-1,3,6-?????????-????(7-hydroxy-1,3,6- naphthalenetrisulfoniacid trisodium salt)? ?? ??? ?? ?, ? ?? 0.5% ????? ??.
????????
??????? ? ? : ????????(???? 238nm)
??????? ? ? : A : ???????(1.54→1,000)
?????????????????B : ??????
????????A?? 5?? ??? ?, A? : B?(100 : 0) → A? : B? (70 : 30) 50?
??(9) ????????1??? : ????? ? ????????1?????? ? ?, ? ?? ?????? 0.01% ????? ??.
????
? (1) ? ?? 0.1g? ? 100mL? ??? ??? ????.
??(2) ? ?? 0.1g? ?? 10mL? ??? ???? ???? ? ? 2～3??? ? 5mL? ??? ???? ????.
??(3) ? ?? 0.1g? ???????(3→2,000) 100mL? ??? ? ? 1mL? ???????(3→2,000)? ??? 100mL? ? ?? ?? 508±2nm? ?????? ??.
???
? ? ?? ? 1.7g? ??? ?? ?? ?? 250mL? ?? ? ? 50mL? ?????? ?? ????? ? ???? ?????? (?)? ?? ????.
0.1N ??????? 1mL = 15.788mg C20H11N2Na3O10S3?1?H2O
??
? ? ??? 4-???-1-???????? ?????? 7-????-1,3-????????? ??? ???? ?, ???? ???? ???? ???? 7-????-8-(4-???????)-1,3-???????????? 1????? ????? ??.
??? ??
Deep red powder?? ??
4-Aminonaphthalene-1-sulfonic acid diazo, and 7-Hydroxynaphthalene-1,3-disulfonic acid coupling.Safety Profile
Moderately toxic by intraperitoneal route. Questionable carcinogen with experimental tumorigenic data. Mutation data reported. When heated to decomposition it emits toxic fumes of NOx and SOx.Purification Methods
Dissolve the dye in the minimum quantity of boiling water, filter and enough EtOH is added to precipitate ca 80% of the dye. This process is repeated until a solution of the dye in aqueous 20% pyridine has a constant extinction coefficient. [Beilstein 16 I 306.]?? ?? 102? ?? ?? ? ???
???
?? ??
?? ?? 102? ?? ??
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