NEO-ALLOOCIMENE, STAB.
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NEO-ALLOOCIMENE, STAB. ??
- ???
- -20.6°C
- ?? ?
- 196-198 °C
- ??
- 0.811 g/mL at 20 °C(lit.)
- ???
- 83Pa at 20℃
- ???
- n20/D 1.546
- ???
- 38 °C
- ?? ??
- 2-8°C
- ???
- 9.38mg/L at 20℃
- LogP
- 4.71 at 25℃
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| ?? ???? ?? | 10 | ||
|---|---|---|---|
| ????(UN No.) | 1993 | ||
| ?? ?? | 3.2 | ||
| ???? | III |
NEO-ALLOOCIMENE, STAB. C??? ??, ??, ??
Purification Methods
Fractionally distil allocimene through an efficient column and repeatedly distil it at 15mm through a long column of glass helices, with a final distillation from sodium under nitrogen. It should be stabilised with ca 0.1% of hydroquinone. UV: max nm( 1cm-1) 290 (32 500), 279 (41 900) and 278 (42,870). [Alder et al. Justus Liebigs Ann Chem 609 1 1957, O’Connor & Goldblatt Anal Chem 26 1726 1954, Beilstein 1 IV 1106.]NEO-ALLOOCIMENE, STAB. ?? ?? ? ???
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NEO-ALLOOCIMENE, STAB. ?? ??
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