ChemicalBook >?? ???? >5-???-2,1,3-??????
5-???-2,1,3-??????
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5-???-2,1,3-?????? ??
- ???
- 72 °C
- ?? ?
- 255.8±32.0 °C(Predicted)
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- 1.826±0.06 g/cm3(Predicted)
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- Room temperature.
- ?? ?? (pKa)
- -1.63±0.36(Predicted)
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- CAS ??????
- 51376-06-8
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5-???-2,1,3-?????? C??? ??, ??, ??
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Triphenylphosphine (1.1 mmol) was dissolved in dry toluene (3 mL) and stirred at 110°C under argon atmosphere; then 6-bromobenzo[c][1,2,5]oxadiazole 1-oxide (1 mmol) in toluene (0.5 mL) was added dropwise over 1 hour and the resulting mixture was stirred for 3 hours. After completion, the solvent was evaporated in vacuo, and the crude was purified through flash column chromatography (cyclohexane - diethyl ether 98:2) to afford 5-Bromobenzo[c][1,2,5]oxadiazole which is a pale pink solid.
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