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1-??-4-??-1,2,3,6-????????????

1-??-4-??-1,2,3,6-????????????
1-??-4-??-1,2,3,6-???????????? ??? ???
?? ??:
23007-85-4
???:
1-??-4-??-1,2,3,6-????????????
???(??):
1-??-4-??-1,2,3,6-????????????
???:
1-Methyl-4-phenyl-1,2,3,6-tetrahydropyridine hydrochloride
???(??):
MPTP;MPTP HCl;MPTP HYDROCHLORIDE;0MPTP hydrochloride;Methyl Hydrochloride;23007-85-4/28289-54-5;NSC 139654 Hydrochloride;Pethidine EP Impurity B HCl;MPTP hydrochloride, 10 mM in DMSO;1-METHYL-4-PHENYL-1 2 3 6-TETRAHYDROPYR&
CBNumber:
CB0133791
???:
C12H16ClN
??? ??:
209.72
MOL ??:
23007-85-4.mol
MSDS ??:
SDS

1-??-4-??-1,2,3,6-???????????? ??

???
249.0 to 254.0 °C
?? ??
Inert atmosphere,Room Temperature
???
DMSO(?? ???), ???(?? ???), ?(?? ???)
??? ??
?? ??
??
???? ?????
???
water: 100mg/mL
BRN
3707312
???
???
InChI
InChI=1S/C12H15N.ClH/c1-13-9-7-12(8-10-13)11-5-3-2-4-6-11;/h2-7H,8-10H2,1H3;1H
InChIKey
KOWJANGMTAZWDT-UHFFFAOYSA-N
SMILES
C1(=CCN(C)CC1)C1C=CC=CC=1.Cl
CAS ??????
23007-85-4
??
  • ?? ? ?? ??
  • ?? ? ???? ?? (GHS)
??? ?? T
?? ???? ?? 25-39/23/24/25-36/37/38
????? 45-39-26
????(UN No.) 2811
WGK ?? 3
RTECS ?? UT8358950
HS ?? 2933.39.9200
?? ?? 6.1(b)
???? III
????(GHS): GHS hazard pictogramsGHS hazard pictograms
?? ?: Danger
??·?? ??:
?? ??·?? ?? ?? ?? ?? ?? ? ?? ?? P- ??
H301 ??? ??? ?? ?? ?? - ?? ?? 3 ?? GHS hazard pictograms P264, P270, P301+P310, P321, P330,P405, P501
H370 ??(??, ??? ?? ??? ?? ??? ??)? ??? ???(????? ?? ???? ??? ???? ???? ???? ????? ??? ????? ??) ?? ???? ?? - 1? ?? ?? 1 ?? GHS hazard pictograms P260, P264, P270, P307+P311, P321,P405, P501
??????:
P260 ??·?·??·???·??·...·????? ???? ???.
P264 ?? ??? ?? ??? ????.
P264 ?? ??? ?? ??? ????.
P270 ? ??? ??? ??? ???, ???? ???? ???.
P301+P310 ???? ?? ????(??)? ??? ????.
P405 ???? ?????.
P501 ...? ??? / ??? ?? ???.

1-??-4-??-1,2,3,6-???????????? C??? ??, ??, ??

??? ??

White Solid

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1-Methyl-4-phenyl-1,2,3,6-tetrahydropyridine hydrochloride is a dopaminergic neurotoxin that reportedly causes a severe and irreversible Parkinsonian condition in humans and monkeys.

Purification Methods

Purify MPTP by recrystallisation from pKEst ~ Me2CO/isoPrOH. The free base has m 40-42o(from heptane), b 99-100o/1.3mm, 128-132o/12mm, (137-142o/0.8mm), n 25 1.5347. The hydrochloride has m 251-252o(from Me2CO/isoPrOH) [Schmidle & Mansfield J Am Chem Soc 78 425 1956, Defeudis Drug Dev Res 15 1 1988, Beilstein 20 III/IV 3240, 20/7 V 121.]

?? ??

[1] Lun-Yi Zang, Hara P Misra. “Inactivation of acetylcholinesterase by 1-methyl-4-phenyl-1,2,3,6-tetrahydropyridine hydrochloride.” Molecular and Cellular Biochemistry 254 1–2 (2003): 131–6.
[2] Gregory L. Willis, Alan D. Robertson. “Recovery from experimental Parkinson’s disease in the 1-methyl-4-phenyl-1,2,3,6-tetrahydropyridine hydrochloride treated marmoset with the melatonin analogue ML-23.” Pharmacology Biochemistry and Behavior 80 1 (2005): Pages 9-26.
[3] Atsushi Fujita. “Connexin 30 deficiency attenuates A2 astrocyte responses and induces severe neurodegeneration in a 1-methyl-4-phenyl-1,2,3,6-tetrahydropyridine hydrochloride Parkinson’s disease animal model.” Journal of Neuroinflammation (2018): 227.

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