4-Nitroperoxybenzoesure Chemische Eigenschaften,Einsatz,Produktion Methoden

Verwenden

4-Nitroperoxybenzoic acid is an electrophile that transfers oxygen to alkenes.

synthetische

The reaction between Na2O2 and p-Nitrobenzoyl Chloride in THF in the  presence of small quantities of water below -5 °C furnishes the sodium salt of PNPBA. p,p′- Dinitrobenzoyl peroxide and p-nitrobenzoic acid are removed from the reaction mixture during  workup. PNPBA (purity 94-96%) is obtained in 85% yield (0.1 mol scale).

Vorbereitung Methode

This peroxide can be prepared from p-nitrobenzoic acid and 90% hydrogen peroxide in methanesulfonic acid medium.

Synthesis Reference(s)

The Journal of Organic Chemistry, 27, p. 1336, 1962 DOI: 10.1021/jo01051a050
Synthetic Communications, 18, p. 2123, 1988 DOI: 10.1080/00397918808068282

4-Nitroperoxybenzoesure Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte

4-Nitroperoxybenzoesure Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Firmenname	Telefon	E-Mail	Land	Produktkatalog	Edge Rate
Shaanxi Dideu Medichem Co. Ltd	+86-29-81148696 +86-15536356810	1022@dideu.com	China	3882	58
Shaanxi DIDU pharmaceutical and Chemical Co., Ltd	029-81120477 17792793610	1033@dideu.com	China	10011	58

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• p-Nitroperbenzoic acid
• 4-nitroperoxybenzoic acid
• 4-nitroperbenzoic acid
• Benzenecarboperoxoic acid, 4-nitro-
• 943-39-5