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(3R,4R)-1-benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride

(3R,4R)-1-benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride Struktur
1062580-52-2
CAS-Nr.
1062580-52-2
Englisch Name:
(3R,4R)-1-benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride
Synonyma:
(3R,4R)-N,4-Dimethyl-1-(phenylmethyl)-3-piperidinamine hydrochloride;TOF30;Tofacitinib-1;Tofatinib Impurity 5;Tofacitinib interMediate A;Tofacitinib intermediate 3;piperidin-3-amine dihydrochL;Tofacitinib Impurity 123 DiHCl;Azilsartan medoxomil impurity351;Tofacitinib Impurity 5 Dihydrochloride
CBNumber:
CB21011155
Summenformel:
C14H23ClN2
Molgewicht:
254.8
MOL-Datei:
Mol file

(3R,4R)-1-benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride Eigenschaften

Schmelzpunkt:
249～251℃
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
L?slichkeit
Aqueous Acid (Slightly), DMSO (Slightly, Heated, Sonicated), Methanol (Slightly)
Aggregatzustand
Solid
Farbe
White to Off-White
InChI
InChI=1/C14H22N2.ClH/c1-12-8-9-16(11-14(12)15-2)10-13-6-4-3-5-7-13;/h3-7,12,14-15H,8-11H2,1-2H3;1H/t12-,14+;/s3
InChIKey
FVRZQLQXDPJADE-WLZBWWFYNA-N
SMILES
C(C1C=CC=CC=1)N1CC[C@@H](C)[C@@H](NC)C1.Cl |&1:10,12,r|
Sicherheit
  • Risiko- und Sicherheitserkl?rung
  • Gefahreninformationscode (GHS)
HazardClass  IRRITANT
HS Code  2933399990
Bildanzeige (GHS) GHS hazard pictograms
Alarmwort Warnung
Gefahrenhinweise
Code Gefahrenhinweise Gefahrenklasse Abteilung Alarmwort Symbol P-Code
H302 Gesundheitssch?dlich bei Verschlucken. Akute Toxizit?t oral Kategorie 4 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P270, P301+P312, P330, P501
Sicherheit
P264 Nach Gebrauch gründlich waschen.
P264 Nach Gebrauch gründlich waschen.
P270 Bei Gebrauch nicht essen, trinken oder rauchen.
P301+P312 BEI VERSCHLUCKEN: Bei Unwohlsein GIFTINFORMATIONSZENTRUM/Arzt/... (geeignete Stelle für medizinische Notfallversorgung vom Hersteller/Lieferanten anzugeben) anrufen.
P330 Mund ausspülen.
P501 Inhalt/Beh?lter ... (Entsorgungsvorschriften vom Hersteller anzugeben) zuführen.

(3R,4R)-1-benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride Chemische Eigenschaften,Einsatz,Produktion Methoden

Verwenden

(3R,4R)-1-benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development processes and chemical production processes.

Synthese

Synthesis_1062580-52-2
TiCl4(0.2g, 1mmol) and NEt3(0.15 g, 1.5 mmol) were added to toluene, and then add 1-benzyl-4-methyl-3-ketone piperidine (20.3 g, 100 mmol) at 35 ℃. The methylamine solution is added to the reaction solution (9.32 g, 120 mmol) and reaction for 4 h, followed by adding NaBH (OAC) 3 (0.32 g, 1.5 mmol) and glacial acetic acid 2 ml. After the reaction is complete, add saturated salt water to wash the reaction mixture. (3R,4R)-1-benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride was obtained after further purification.

(3R,4R)-1-benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride Upstream-Materialien And Downstream Produkte

Upstream-Materialien

(3R,4R)-1-Benzyl-N,4-dimethylpiperidin-3-amine 1-BENZYL-N,4-DIMETHYLPIPERIDIN-3-AMINE DIHYDROCHLORIDE 1-benzyl-4-methylpiperidin-3-one (1-Benzyl-4-Methyl-1,2,5,6-tetrahydropyridin-3-yl)carbaMic acid Methyl ester Methanamine Acetate 3-Amino-4-methylpyridine

Downstream Produkte

(3R,4R)-1-benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Global( 359)Lieferanten
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  • CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE)
  • cis-1-Benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride
  • cis-1-Benzyl-4-methyl-3-(methylamino)piperidine dihydrochloride 95+%
  • cis-1-Benzyl-N3,4-dimethylpiperidin-3-amine dihydrochloride
  • (3R,4R)-1-BENZYL-N,4-DIMETHYLPIPERIDIN-3-AMINE DIHYDROCHLORIDE
  • (3R,4R)-1-benzyl-N,4-diMethylpiperidin-3-aMine BIS-(HYDROCHLORIDE)
  • 3-PiperidinaMine, N,4-diMethyl-1-(phenylMethyl)-, hydrochloride (1:2), (3R,4R)-
  • (3R,4R)-N,4-DiMethyl-1-(phenylMethyl)-3-piperidi
  • (3R,4R)- Cis-1-benzyl-4-Methyl-3-(MethylaMino)piperidine
  • Tofacitinib interMediate A
  • (3R,4R)- cis-1-Benzyl-4-Methyl-3-(MethylaMino)piperidine dihydrochloride
  • (3R,4R)-1-BENZYL-N,4-DIMETHYLPIPERIDIN-3-AMINE DIHYDROCHLORID
  • 3-Piperidinamine, N,4-dimethyl-1-(phenylmethyl)-, dihydrochloride, (3R,4R)-
  • Tofacitinib intermediate 3
  • (3R,4R)-(1-Benzyl-4-methyl-piperidin-3-yl)-methyl-amine dihydrochloride
  • Azilsartan medoxomil impurity351
  • (3R,4R)-N,4-Dimethyl-1-(phenylmethyl)-3-piperidinamine hydro...
  • Tofacitinib Impurity 5 Dihydrochloride
  • N-((3R,4R)-N,4-Dimethyl-1-(phenylmethyl)-3-piperidinamine hydrochloride
  • (3R,4R)-1-BENZYL-N,4-DIMETHYLPIPERIDIN-3-AMINE 2HCL
  • (3R,4R)-1-BENZYL-N,4-DIMETHYLPIPERIDIN-3-AMINEDITYDROCHLORIDE
  • Cis-n-benzyl-3-methylamino-4-methyl-piperidine bis-(, HCl )
  • (3R,?4R)?-N,?4-?Dimethyl-?1-?(phenylmethyl)?-3-?piperidinamine Dihydrochloride
  • piperidin-3-amine dihydrochL
  • (3R,4R)-N,4-Dimethyl-1-(phenylmethyl)-3-piperidinamine, hydrochloride (1:2)
  • Cis 1-benzyl-4-methyl-3-methylamino-piperidine hydrochloride
  • Tofacitinib-1
  • TOF30
  • (3R,4R)-1-Benzyl-3-(methylamino)-4-methylpiperidine Dihydrochloride
  • (3R,4R)-N,4-Dimethyl-1-(phenylmethyl)-3-piperidinamine HCl
  • (3R,4R)-N,4-Dimethyl-1-(phenylmethyl)-3-piperidinamine hydrochloride
  • (3R,4R)-N, 4-dimethyl-1 -(phenylmethyl) -3-piperidamine hydrochloride
  • Tofatinib Impurity 5
  • (3R,4R)-N,4-Dimethy1-(phenylmethyl)-3-piperidinamine hydrochloride
  • CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE) Tofacitinib （Int.）
  • Tofacitinib Impurity 123 DiHCl
  • (3R,4R)-N,4-Dimethyl-1-(benzyl)-3-piperidinamine 2HCl
  • (3R,4R)-1-Benzyl-N,4-dimethyl-3-piperidinamine dihydrochloride
  • 1062580-52-2
  • C14H22N22HCl
  • 1
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