Allyl triflate Chemische Eigenschaften,Einsatz,Produktion Methoden
Synthesis Reference(s)
The Journal of Organic Chemistry, 42, p. 3109, 1977
DOI: 10.1021/jo00439a001
Synthese
Allyl triflate is prepared by the reaction of Trifluoromethanesulfonic Anhydride (1
equiv) and allyl alcohol (1 equiv) in the presence of pyridine (1 equiv) in carbon tetrachloride at 0 °C.
1 The
insoluble pyridine salt is removed by filtration through sodium sulfate, and the resulting solution is used
directly for allylation reactions. The yield of the reaction is reported to be 75 ± 5% based on quantitative
NMR analysis of aliquots.
Allyl triflate Upstream-Materialien And Downstream Produkte
Upstream-Materialien
Downstream Produkte