2,3,4,9-Tetrahydro-1H-pyrido[3,4-b]indol-1-on Chemische Eigenschaften,Einsatz,Produktion Methoden

synthetische

Tryptamine 380 (9.0 g, 56.2 mmol) and triethylamine (13.8 g, 136.3 mmol) were dissolved in warm toluene (800 mL). Under vigorous stirring, a solution of triphosgene (6.7 g, 22.6 mmol) in toluene (35 mL) was added dropwise and the mixture was stirred for a further 20 min at room temperature. Then, HBr (30% in acetic acid; 13 mL) was added and the mixture was refluxed for 30 min. After cooling to room temperature, water (300 mL) and ethyl acetate (300 mL) were added and, after separation of the layers, the aqueous phase was extracted once more with ethyl acetate (300 mL). The combined organic layers were dried over magnesium sulfate and concentrated in vacuo. The residue was recrystallized from methanol/ethyl acetate (1:1) to afford 7.74 g (74%) of 2,3,4,9-tetrahydro-1H-pyrido[ 3,4-b]indol-1-one 382 as a white solid; mp 184°C.

2,3,4,9-Tetrahydro-1H-pyrido[3,4-b]indol-1-on Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte

2,3,4,9-Tetrahydro-1H-pyrido[3,4-b]indol-1-on Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Firmenname	Telefon	E-Mail	Land	Produktkatalog	Edge Rate
Accela ChemBio Inc.	+1-858-6993322	info@accelachem.com	United States	17836	58
TargetMol Chemicals Inc.	+1-781-999-5354 +1-00000000000	marketing@targetmol.com	United States	32161	58
TargetMol Chemicals Inc.		support@targetmol.com	United States	38631	58
Amadis Chemical Company Limited	571-89925085	sales@amadischem.com	China	131957	58
Accela ChemBio Co.,Ltd.	021-50795510 4000665055	sales@accelachem.com	China	11655	64
Shanghai Tombiopharma Chemical Co. Ltd.	13391076197	tombiopharma@163.com	China	4987	55
Wuhan ChemFaces Biochemical Co., Ltd.	18607101326 15172504745	aileen@chemfaces.com	China	6905	55
EMMX Biotechnology LLC	888-539-0666	info@emmx.com	United States	8447	60
Shanghai YuanYe Biotechnology Co., Ltd.	021-61312847; 18021002903	3008007409@qq.com	China	27313	60
Aikon International Limited	025-58851090 13611564524	lwan@aikonchem.com	China	15951	58

17952-82-8(2,3,4,9-Tetrahydro-1H-pyrido[3,4-b]indol-1-on)Verwandte Suche:

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• 2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-one
• 1,2,3,4-Tetrahydro-β-carboline-1-one
• 3,4-Dihydro-β-carboline-1(2H)-one
• 1,2,3,4-Tetrahydronorharman-1-one
• 1H-Pyrido[3,4-b]indol-1-one, 2,3,4,9-tetrahydro-
• 2,3,4,9-tetrahydropyrido[3,4-b]indol-1-one
• 17952-82-8