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ChemicalBook--->CAS DataBase List--->869494-16-6

869494-16-6

869494-16-6 Structure

869494-16-6 Structure
IdentificationBack Directory
[Name]

3,6-Diazabicyclo[3.1.1]heptane-6-carboxylic acid tert-butyl ester
[CAS]

869494-16-6
[Synonyms]

3,6-DiazabicycL
o[3.1.1]heptane-6-carboxyL
6-Boc-3,6-diaza-bicyclo[3.1.1]heptane
tert-Butyl 3,6-diazabicyclo[3.1.1]heptane-6-carboxylate
6-(tert-Butyloxycarbonyl)-3,6-diazabicyclo[3.1.1]heptane
tert-Butyl 3,6-diazabicyclo[3.1.1]heptane-6-carboxylate 97%
(1R,5S)-tert-butyl 3,6-diazabicyclo[3.1.1]heptane-6-carboxylate
tert-Butyl (1S,5R)-3,6-diazabicyclo[3.1.1]heptane-6-carboxylate
3,6-Diazabicyclo[3.1.1]heptane-6-carboxylic acid tert-butyl ester
3,6-Diazabicyclo[3.1.1]heptane-6-carboxylic acid, 1,1-dimethylethyl ester
3,?6-?Diazabicyclo[3.1.1]?heptane-?6-?carboxylic acid, 1,?1-?dimethylethyl ester 869494-16-6
[Molecular Formula]

C10H18N2O2
[MDL Number]

MFCD17016736
[MOL File]

869494-16-6.mol
[Molecular Weight]

198.26
Chemical PropertiesBack Directory
[Boiling point ]

276℃
[density ]

1.104
[Fp ]

121℃
[storage temp. ]

Keep in dark place,Sealed in dry,2-8°C
[form ]

solid
[pka]

9.53±0.20(Predicted)
[color ]

White to off-white
[InChI]

InChI=1S/C10H18N2O2/c1-10(2,3)14-9(13)12-7-4-8(12)6-11-5-7/h7-8,11H,4-6H2,1-3H3
[InChIKey]

OUFBVDKNEWUFHP-UHFFFAOYSA-N
[SMILES]

C12CC(N1C(OC(C)(C)C)=O)CNC2
Safety DataBack Directory
[Symbol(GHS) ]


GHS07
[Signal word ]

Warning
[Hazard statements ]

H302+H312+H332-H315-H319-H335
[Precautionary statements ]

P280-P301+P312-P261
[HS Code ]

2933599590
Spectrum DetailBack Directory
[Spectrum Detail]

3,6-Diazabicyclo[3.1.1]heptane-6-carboxylic acid tert-butyl ester(869494-16-6)1HNMR
Hazard InformationBack Directory
[Synthesis]

To a stirred solution of 3,6-Diazabicyclo[3.1.1]heptane-6-carboxylic acid, 3-[(2-nitrophenyl)sulfonyl]-, 1,1-dimethylethyl ester (400 mg, 1.04 mmol) in DMF (2.5 mL) were added dodecanethiol (500 μL, 2.09 mmol) and lithium hydroxide hydrate (88 mg, 2.09 mmol). The mixture was stirred at r.t. for 2 h. The mixture was diluted with hexanes-ethyl acetate (10 mL, 1:1). The mixture was extracted with aq. Hydrochloric acid (2 x 5.0 mL). The aq. layer was extracted with hexanes-ethyl acetate (10 mL, 1:1). The combined organic layers were discarded. The aq. layer was basified with NaOH (6.0 mL of 1.0 M solution) until pH=13. The aq. layer was extracted with methylene chloride-methanol (2 x 10 mL, 9:1). The organic layer was washed with brine, dried over anhydrous magnesium sulfate, filtered and concentrated in vacuo to afford tert-Butyl 3,6-diazabicyclo[3.1.1]heptane-6-carboxylate as a white solid; Yield, 167 mg (81percent)
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