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ChemicalBook--->CAS DataBase List--->63503-60-6

63503-60-6

63503-60-6 Structure

63503-60-6 Structure
IdentificationMore
[Name]

3-Chlorophenylboronic acid
[CAS]

63503-60-6
[Synonyms]

3-CHLOROBENZENEBORONIC ACID
3-CHLOROPHENYLBORNIC ACID
3-CHLOROPHENYLBORONIC ACID
AKOS BRN-0010
M-CHLOROPHENYLBORONIC ACID
RARECHEM AH PB 0179
3-CHLOROBENZENEBORONIC ACID/3-CHLOROPHENYLBORONIC ACID
3-CHLOROPHENYLBORONIC ACID 98%
3-Chlorophenylboronic Acid (contains varying amounts of Anhydride)
[EINECS(EC#)]

628-786-6
[Molecular Formula]

C6H6BClO2
[MDL Number]

MFCD00161354
[Molecular Weight]

156.37
[MOL File]

63503-60-6.mol
Chemical PropertiesBack Directory
[Appearance]

white to light yellow-green crystalline powder or
[Melting point ]

185-189 °C(lit.)
[Boiling point ]

311.4±44.0 °C(Predicted)
[density ]

1.32±0.1 g/cm3(Predicted)
[storage temp. ]

0-6°C
[solubility ]

soluble in Methanol
[form ]

Crystalline Powder or Needles
[pka]

7.55±0.10(Predicted)
[color ]

White to light yellow-green
[Water Solubility ]

Slightly soluble in water. soluble in ether, tetrahydrofuran,, dimethyl sulfoxide, dimethyl formamide, methanol.
[BRN ]

2936343
[InChI]

InChI=1S/C6H6BClO2/c8-6-3-1-2-5(4-6)7(9)10/h1-4,9-10H
[InChIKey]

SDEAGACSNFSZCU-UHFFFAOYSA-N
[SMILES]

B(C1=CC=CC(Cl)=C1)(O)O
[CAS DataBase Reference]

63503-60-6(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

Xn,Xi
[Risk Statements ]

R20/21/22:Harmful by inhalation, in contact with skin and if swallowed .
R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S36:Wear suitable protective clothing .
S37/39:Wear suitable gloves and eye/face protection .
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
[WGK Germany ]

3
[Hazard Note ]

Irritant
[HazardClass ]

IRRITANT
[HS Code ]

29319099
Hazard InformationBack Directory
[Chemical Properties]

white to light yellow-green crystalline powder or
[Uses]

suzuki reaction
[Synthesis]

Using m-dichlorobenzene as the starting material, iodine particles and 1,2-dibromoethane as the initiator reacts with magnesium in an organic solvent to prepare 3-chlorophenyl magnesium chloride. Then, the trimethyl borate is reacted with an organic solvent to prepare 3-chlorophenyl borate dimethyl ester. Finally, the product 3-chlorophenylboronic acid is obtained through hydrolysis, extraction, and crystallization.
[Solubility in organics]

3-Chlorophenylboronic acid can be dissolved in organic solvents such as N, N-dimethylformamide, ethyl acetate, and dichloromethane. In addition, it also has specific solubility in low-polarity and non-polar organic solvents, but 3-chlorophenylboronic acid has poor solubility in water.
Spectrum DetailBack Directory
[Spectrum Detail]

3-Chlorophenylboronic acid(63503-60-6)1HNMR
3-Chlorophenylboronic acid(63503-60-6)IR
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

3-Chlorophenylboronic acid, 97%(63503-60-6)
[Alfa Aesar]

3-Chlorobenzeneboronic acid, 97%(63503-60-6)
[Sigma Aldrich]

63503-60-6(sigmaaldrich)
[TCI AMERICA]

3-Chlorophenylboronic Acid  (contains varying amounts of Anhydride)(63503-60-6)
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