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ChemicalBook--->CAS DataBase List--->26164-26-1

26164-26-1

26164-26-1 Structure

26164-26-1 Structure
IdentificationMore
[Name]

(S)-(+)-alpha-Methoxyphenylacetic acid
[CAS]

26164-26-1
[Synonyms]

O-METHYL-L-MANDELIC ACID
(S)-(+)-ALPHA-METHOXYPHENYLACETIC ACID
(S)-ALPHA-METHOXYPHENYLACETIC ACID
(S)-(+)-A-METHOXYPHENYLACETIC ACID
(S)-(+)-METHOXYPHENYLACETIC ACID
Methoxy(phenyl)acetic acid
(S)-(+)-A-METHOXYPHENYLACETIC ACID FLU&
O-Methyl-(S)-mandelicacid
(s)-(+)-à-methoxyphenylacetic acid
(S)-(+)-ALPHA-METHOXYPHENYLACETIC ACID 99%
(S)-(+)-ɑ-Methoxyphenylacetic acid, 99%
(2S)-2-Methoxy-2-phenylacetic acid
(S)-α-Methoxybenzeneacetic acid
(αS)-α-Methoxybenzeneacetic acid
[S,(+)]-α-Methoxybenzeneacetic acid
[EINECS(EC#)]

247-492-5
[Molecular Formula]

C9H10O3
[MDL Number]

MFCD00064216
[Molecular Weight]

166.17
[MOL File]

26164-26-1.mol
Chemical PropertiesBack Directory
[Appearance]

White Solid
[Melting point ]

64-66 °C(lit.)
[alpha ]

160 º (C=1, MEOH)
[Boiling point ]

164-166°C 18mm
[density ]

1.1708 (rough estimate)
[refractive index ]

147 ° (C=0.5, EtOH)
[Fp ]

164-166°C/18mm
[storage temp. ]

Sealed in dry,Room Temperature
[solubility ]

Chloroform (Slightly), Ethanol (Slightly)
[form ]

Fine Crystalline Powder or Crystals
[pka]

3.10±0.10(Predicted)
[color ]

White
[optical activity]

[α]17/D +150°, c = 1 in ethanol
[Water Solubility ]

Soluble
[BRN ]

2361718
[CAS DataBase Reference]

26164-26-1(CAS DataBase Reference)
[NIST Chemistry Reference]

Benzeneacetic acid, «alpha»-methoxy-, (s)-(26164-26-1)
Safety DataBack Directory
[Hazard Codes ]

Xi
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36:Wear suitable protective clothing .
[WGK Germany ]

3
[HS Code ]

29189900
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Ethanol-->Methanol-->Sulfuric acid-->Thionyl chloride-->PETROLEUM ETHER-->Chloroform-->Magnesium sulfate-->Sodium chloride-->Iodomethane-->Silver oxide-->CALCIUM SULFATE-->(S)-(+)-Mandelic acid
Hazard InformationBack Directory
[Chemical Properties]

White Solid
[Uses]

(S)-(+)-α-Methoxyphenylacetic Acid (cas# 26164-26-1) is a compound useful in organic synthesis.
[Uses]

Reactant involved in the synthesis of biologically active molecules including:
  • Acyclonucleoside phosphonates structural analogs of adefovir
  • Labeled discodermolide for studying binding to tubulin
  • 10-Isocyano-4-cadinene used for antifouling activity

Reactant involved in studies of immunostimulating chromanones gonytolides A-C

Reactant involved in:
  • Hydroxylations and epoxidations
  • Hydrogenations
[Purification Methods]

Purify the acids by recrystallising from *C6H6/pet ether (b 80-100o). [Neilson & Peters J Chem Soc 1519 1962, Weizmann et al. J Am Chem Soc 70 1153 1948, Pirie & Smith J Chem Soc 338 1932, NMR: Dale & Mosher J Am Chem Soc 9 5 512 1973, for resolution: Roy & Deslongchamps Can J Chem 63 651 1985, Trost et al. J Am Chem Soc 1 0 8 4974 1986.] The racemic mixture has m 72o, b 121-122o/0.4mm, 165o/18mm (from pet ether) [Braun et al. Chem Ber 6 3 2847 1930]. [Beilstein 10 IV 566.]
Spectrum DetailBack Directory
[Spectrum Detail]

(S)-(+)-alpha-Methoxyphenylacetic acid(26164-26-1)1HNMR
(S)-(+)-alpha-Methoxyphenylacetic acid(26164-26-1)Raman
(S)-(+)-alpha-Methoxyphenylacetic acid(26164-26-1)FT-IR
(S)-(+)-alpha-Methoxyphenylacetic acid(26164-26-1)IR
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

(S)-(+)-alpha-Methoxyphenylacetic acid, 99%(26164-26-1)
[Alfa Aesar]

(S)-(+)-alpha-Methoxyphenylacetic acid, 99%(26164-26-1)
[Sigma Aldrich]

26164-26-1(sigmaaldrich)
[TCI AMERICA]

(S)-(+)-alpha-Methoxyphenylacetic Acid,>98.0%(GC)(T)(26164-26-1)
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