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ChemicalBook--->CAS DataBase List--->1500-85-2

1500-85-2

1500-85-2 Structure

1500-85-2 Structure
IdentificationMore
[Name]

4-Amino-7H-pyrrolo[2,3-d]pyrimidine
[CAS]

1500-85-2
[Synonyms]

4-AMINOPYRROLO[2,3-D]PYRIMIDINE
7-DEAZAADENINE
7H-PYRROLO[2,3-D]PYRIMIDIN-4-AMINE
3-d)pyrimidine,4-amino-7h-pyrrolo(
4-Amino-7H-pyrrolo[2,3-d]pyrimidine
1H-Pyrrolo[2,3-d]pyrimidin-4-amine (9CI)
4-Aminopyrrolo[2,3-d]Pyrimidin
4-AMINO-7H-PYRROLO[2,3-D]PYRIMIDINE SULFATE 98%
[Molecular Formula]

C6H6N4
[MDL Number]

MFCD01686848
[Molecular Weight]

134.14
[MOL File]

1500-85-2.mol
Chemical PropertiesBack Directory
[Melting point ]

257-262℃
[Boiling point ]

318.3±45.0 °C(Predicted)
[density ]

1.61±0.1 g/cm3(Predicted)
[storage temp. ]

Keep in dark place,Inert atmosphere,2-8°C
[form ]

Solid
[pka]

13.38±0.20(Predicted)
[color ]

White to pale brown
[Sensitive ]

Moisture & Light Sensitive
[InChIKey]

PEHVGBZKEYRQSX-UHFFFAOYSA-N
[CAS DataBase Reference]

1500-85-2(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

T
[Risk Statements ]

25
[Safety Statements ]

45
[RIDADR ]

UN 2811 6.1/PG 1
[WGK Germany ]

2
[RTECS ]

UY8850000
[HazardClass ]

IRRITANT
[PackingGroup ]

[HS Code ]

2933599590
[Toxicity]

mouse,LD50,intraperitoneal,300mg/kg (300mg/kg),Gann. Japanese Journal of Cancer Research. Vol. 56, Pg. 219, 1965.
Spectrum DetailBack Directory
[Spectrum Detail]

4-Amino-7H-pyrrolo[2,3-d]pyrimidine(1500-85-2)1HNMR
Hazard InformationBack Directory
[Synthesis]

A mixture of 5-ethynylpyrimidine-4,6-diamine (300?mg, 2.24?mmol), Cs2CO3 (1.46?g, 4.47?mmol) and DMSO (4.00?ml) in a 10.00?ml microwave tube was irradiated at 100?W and 180?°C for 15?minutes. After this time, the reaction mixture was cooled to room temperature and poured into a separating funnel containing 100?ml water and 100?ml ethyl acetate. The aqueous layer was extracted with EtOAc (2×100?ml). The combined organic extracts were dried with MgSO4 and filtered through celite, and excess solvent was removed in vacuo. Purification by column chromatography (80?% EtOAc/hexane – 10?% MeOH/CH2Cl2) gave 7H-pyrrolo[2,3-d]pyrimidin-4-amine (4-Amino-7H-pyrrolo[2,3-d]pyrimidine) (0.15?g, 50?%) as an off-white solid[1].
[References]

[1] Dr. Tswene D. Seanego. “7H-Pyrrolo[2,3-d]pyrimidine-4-amines as Potential Inhibitors of Plasmodium falciparum Calcium-Dependent Protein Kinases.” ChemMedChem 17 22 (2022).
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