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ChemicalBook--->CAS DataBase List--->139-66-2

139-66-2

139-66-2 Structure

139-66-2 Structure
IdentificationMore
[Name]

Diphenyl sulfide
[CAS]

139-66-2
[Synonyms]

DIPHENYL SULFIDE
DIPHENYL SULPHIDE
PHENYL SULFIDE
PHENYL SULPHIDE
(Phenylsulfanyl)benzene
1,1’-thiobis(benzene)
1,1’-Thiobis[benzene]
1,1’-thiobis-benzen
1,1'-Thiobis(benzene)
Benzene, 1,1'-thiobis-
benzene,1,1’-thiobis
Diphenyl monosulfide
Diphenyl thioether
Diphenylmercaptan
Diphenylthiamethane
diphenylthioether
Phenylthiobenzene
Sulfide, diphenyl
sulfide,diphenyl
Diphenyl sulphide 99%
[EINECS(EC#)]

205-371-4
[Molecular Formula]

C12H10S
[MDL Number]

MFCD00003064
[Molecular Weight]

186.27
[MOL File]

139-66-2.mol
Chemical PropertiesBack Directory
[Appearance]

colourless liquid
[Melting point ]

-40 °C (lit.)
[Boiling point ]

296 °C (lit.)
[density ]

1.113 g/mL at 20 °C(lit.)
[vapor pressure ]

0.01 hPa (25 °C)
[refractive index ]

n20/D 1.6327(lit.)
[Fp ]

>230 °F
[storage temp. ]

Store below +30°C.
[solubility ]

Soluble in ether, benzene, carbon disulphide.
[form ]

Liquid
[color ]

Clear colorless to light yellow
[Stability:]

Stable. Combustible. Incompatible with strong oxidizing agents.
[Water Solubility ]

insoluble
[Sensitive ]

Stench
[Merck ]

14,7314
[BRN ]

1907932
[InChIKey]

LTYMSROWYAPPGB-UHFFFAOYSA-N
[CAS DataBase Reference]

139-66-2(CAS DataBase Reference)
[NIST Chemistry Reference]

Diphenyl sulfide(139-66-2)
[EPA Substance Registry System]

139-66-2(EPA Substance)
Safety DataBack Directory
[Hazard Codes ]

Xn,N
[Risk Statements ]

R22:Harmful if swallowed.
R38:Irritating to the skin.
R50/53:Very Toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment .
R36/38:Irritating to eyes and skin .
[Safety Statements ]

S23:Do not breathe gas/fumes/vapor/spray (appropriate wording to be specified by the manufacturer) .
S28:After contact with skin, wash immediately with plenty of ... (to be specified by the manufacturer) .
S60:This material and/or its container must be disposed of as hazardous waste .
S61:Avoid release to the environment. Refer to special instructions safety data sheet .
S37/39:Wear suitable gloves and eye/face protection .
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
[RIDADR ]

UN 3082 9/PG 3
[WGK Germany ]

3
[RTECS ]

SX2275000
[F ]

13
[Hazard Note ]

Harmful/Stench
[TSCA ]

Yes
[HazardClass ]

6.1
[PackingGroup ]

III
[HS Code ]

29309090
[Toxicity]

LD50 orally in rats: 0.49 ml/kg (Smyth)
Raw materials And Preparation ProductsBack Directory
[Raw materials]

ZINC-->Disulfur dichloride-->Phenyl sulfoxide
[Preparation Products]

2,4-Dichlorophenol-->2-Chlorothioxanthone-->2-CHLORO-9-(3-(DIMETHYLAMINO)PROPYL)-TH&-->4-Hydroxylthiocoumarin-->Fenticonazole nitrate-->2,3-DIBROMOPHENOL-->4-Thiophenyl phenyl diphenyl sulfonium hexafluoroantimonate-->DIPHENYL(METHYL)SULFONIUM TETRAFLUOROBORATE-->4-CHLOROPHENYL SULFOXIDE-->Thianthrene-->p-(phenylthio)benzyl alcohol-->4,4'-Thiodibenzenethiol-->Phenylsulfenylchloride
Hazard InformationBack Directory
[Chemical Properties]

colourless liquid
[Uses]

Diphenyl Sulfide is an aromatic organosulfur compound. Diphenyl Sulfide is metabolite of the fungicide Edifenphos as well as a potential Impurity of Fenticonazole Nitrate (F279250).
[Definition]

ChEBI: An aryl sulfide that consists of two phenyl groups connected by a sulphur atom.
[Synthesis Reference(s)]

Chemical and Pharmaceutical Bulletin, 35, p. 1770, 1987 DOI: 10.1248/cpb.35.1770
[Flammability and Explosibility]

Notclassified
[Purification Methods]

Wash the sulfide with aqueous 5% NaOH, then water. Dry it with CaCl2, then with sodium. The sodium is filtered off, and the diphenyl sulfide is distiiled under reduced pressure. [Beilstein 2 H 299, 6 IV 1488.]
Spectrum DetailBack Directory
[Spectrum Detail]

Diphenyl sulfide(139-66-2)MS
Diphenyl sulfide(139-66-2)1HNMR
Diphenyl sulfide(139-66-2)13CNMR
Diphenyl sulfide(139-66-2)IR1
Diphenyl sulfide(139-66-2)Raman
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

Phenyl sulfide, 99%(139-66-2)
[Alfa Aesar]

Diphenyl sulfide, 98%(139-66-2)
[Sigma Aldrich]

139-66-2(sigmaaldrich)
[TCI AMERICA]

Phenyl Sulfide,>98.0%(GC)(139-66-2)
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