Z-PRO-LEU-ALA-NHOH synthesis
- Product Name:Z-PRO-LEU-ALA-NHOH
- CAS Number:123984-00-9
- Molecular formula:C22H32N4O6
- Molecular Weight:448.51
15761-39-4
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: triethylamine (TEA), dicyclohexylcarbodiimide (DCC), N-hydroxybenzotriazole (HOBt) / dimethylformamide; CH2Cl2 / 5 °C
2: 81 percent / H2 / 5percent Pd-C / methanol / 1 h / Ambient temperature
3: HCl / ethyl acetate / 1 h
4: 70 percent / Triethylamine (TEA) / dimethylformamide / a.) -70 deg C to -10 deg C; b.) 4 deg C
References:
Odake;Okayama;Obata;Morikawa;Hattori;Hori;Nagai [Chemical and Pharmaceutical Bulletin,1990,vol. 38,# 4,p. 1007 - 1011]
13139-15-6
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![L-Alaninamide, N-[(1,1-dimethylethoxy)carbonyl]-L-leucyl-N-(phenylmethoxy)- (9CI)](/CAS/20210305/GIF/123984-16-7.gif)
123984-16-7
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123984-00-9
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