Trityl Olmesartan Medoxomil synthesis
- Product Name:Trityl Olmesartan Medoxomil
- CAS Number:1020157-01-0
- Molecular formula:C48H44N6O6
- Molecular Weight:800.9
58954-23-7
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1020157-01-0
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$145.00/10mg
Yield:-
Steps:
Multi-step reaction with 5 steps
1: 86 percent / HCl / Ambient temperature
2: 95 percent / diethyl ether; CH2Cl2 / 1 h / 10 - 15 °C
3: 1.) t-BuOK / 1.) DMA, 0 deg C, 10 min, 2.) DMA, RT, 1 h
4: LiOH*H2O / dioxane; H2O / 20 h / Ambient temperature
5: 88 percent / K2CO3 / N,N-dimethyl-acetamide / 4 h / 20 - 50 °C
References:
Yanagisawa, Hiroaki;Amemiya, Yoshiya;Kanazaki, Takuro;Shimoji, Yasuo;Fujimoto, Koichi;Kitahara, Yoshiko;Sada, Toshio;Mizuno, Makoto;Ikeda, Masahiro;Miyamoto, Shuichi;Furukawa, Youji;Koike, Hiroyuki [Journal of Medicinal Chemistry,1996,vol. 39,# 1,p. 323 - 338]
752179-89-8
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80841-78-7
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1020157-01-0
63 suppliers
$145.00/10mg
80841-78-7
530 suppliers
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172875-59-1
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133051-88-4
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144689-93-0
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$16.00/5g
1020157-01-0
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1048948-16-8
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80841-78-7
530 suppliers
$10.00/250mg
1020157-01-0
63 suppliers
$145.00/10mg