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ChemicalBook CAS DataBase List Trithiazyl Trichloride
5964-00-1

Trithiazyl Trichloride synthesis

5synthesis methods
-

Yield:5964-00-1 66%

Reaction Conditions:

in tetrachloromethane;mechanism discussed; detailed description of apparatus and handling given; introduction of dry Cl2; N2 atm. (exclusion of moisture); storage (12 h);; pptn.; recrystn. from CCl4;;

References:

[Gmelin Handbuch der Anorganischen Chemie,Gmelin Handbook: S: MVol.B3, 150, page 1847 - 1849] Meuwsen, A. [Silicium, Schwefel, Phosphate, IUPAC Colloquium Muenster/Westf. 1954, Weinheim/Bergstr. 1955, S. 130/2]