TRIS-(4-AMINOPHENYL)THIOPHOSPHATE synthesis
- Product Name:TRIS-(4-AMINOPHENYL)THIOPHOSPHATE
- CAS Number:52664-35-4
- Molecular formula:C18H18N3O3PS
- Molecular Weight:387.39
123-30-8
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: tetrahydrofuran / 30 h
2: triethylamine; phosphorus trichloride / toluene / 24 h / 0 - 20 °C / Inert atmosphere
3: sulfur / 30 h / Inert atmosphere; Reflux
4: trifluoroacetic acid / dichloromethane / 4 h
References:
Butler, Patrick W. V.;Kruger, Paul E.;Ward, Jas S. [Chemical Communications,2019,vol. 55,# 69,p. 10304 - 10307]
![Acetamide, N,N',N''-[phosphinothioylidynetris(oxy-4,1-phenylene)]tris-](/CAS/20240320/GIF/75144-41-1.gif)
75144-41-1
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52664-35-4
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54840-15-2
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