ChemicalBook CAS DataBase List TRIPROPYLPHOSPHINE

TRIPROPYLPHOSPHINE synthesis

6synthesis methods

Product Name:TRIPROPYLPHOSPHINE
CAS Number:2234-97-1
Molecular formula:C9H21P
Molecular Weight:160.24

187737-37-7 Synthesis

187737-37-7
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2234-97-1
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Yield: 97.5%

Reaction Conditions:

with phosphan;zinc(II) oxide in acetone at 0; for 12 h;Irradiation;Solvent;Reagent/catalyst;Temperature;

Steps:

1-8
Add acetone solution and 0.01 mol ZnO powder to the transparent reactor, stir well, then slowly flush 1 mol phosphine and 5 mol propylene into the reactor, fully stir, use a 50W energy-saving lamp to react at 0°C under white light irradiation, the reaction time is 12h, After the completion of the reaction, the catalyst was removed by filtration and distilled under reduced pressure to obtain tripropyl phosphine with a yield of 97.5% (calculated as phosphine) and a purity of 96.2%.

References:

Shandong Zhuojun Industrial Co., Ltd.;Li Juan CN111995641, 2020, A Location in patent:Paragraph 0044-0059