TRIMETHYLSILYLMETHYLMAGNESIUM CHLORIDE synthesis
- Product Name:TRIMETHYLSILYLMETHYLMAGNESIUM CHLORIDE
- CAS Number:13170-43-9
- Molecular formula:C4H11ClMgSi
- Molecular Weight:146.97
7439-95-4
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$11.60/0.9g
2344-80-1
289 suppliers
$15.00/1g
13170-43-9
163 suppliers
$45.00/1mL
Yield:-
Reaction Conditions:
in tetrahydrofuran at 20; for 3 h;
Steps:
52
Example 52; (Trimethylsilyl)methylmagnesium chloride; To a well-stirred mixture of magnesium turnings (3.75 g, 154.04 mmol) in 120 mL of THF was added (chloromethyl)trimethylsilane (9.44 g, 77.02 mmol) in 37 mL of THF. The mixture was stirred for 3 h at room temperature to ensure complete generation of the organomagnesium species and was then used fresh.
References:
Isis Innovation Limited US2007/142632, 2007, A1 Location in patent:Page/Page column 35
2344-80-1
289 suppliers
$15.00/1g
13170-43-9
163 suppliers
$45.00/1mL