TRIMETHYLSILYL-N N-DIPHENYLUREA synthesis
2synthesis methods
- Product Name:TRIMETHYLSILYL-N N-DIPHENYLUREA
- CAS Number:1154-84-3
- Molecular formula:C16H20N2OSi
- Molecular Weight:284.43
Yield:1154-84-3 56%
Reaction Conditions:
in pentane at -0.16 - 19.84;Inert atmosphere;
Steps:
General procedure for the synthesis of ureaylsilanes 13-24 (C)
General procedure: To a solution of the aminosilane in n-pentane, stirredat 273 K, the appropriate amount of phenylisocyanatewas added dropwise through a syringe. The solutionwas stirred overnight at room temperature. Thereafter,volatiles were removed in vacuo.
References:
Kraushaar, Konstantin;Herbig, Marcus;Schmidt, Dana;Wagler, J?rg;B?hme, Uwe;Kroke, Edwin [Zeitschrift fur Naturforschung, B: Chemical Sciences,2017,vol. 72,# 11,p. 909 - 921]
