Triethylamine hydrochloride synthesis
- Product Name:Triethylamine hydrochloride
- CAS Number:554-68-7
- Molecular formula:C6H16ClN
- Molecular Weight:137.65
96-45-7
460 suppliers
$7.00/25g
554-68-7
484 suppliers
$6.00/25g
Yield:554-68-7 97%
Reaction Conditions:
with triethylamine in tetrahydrofuran;
Steps:
147.B B.
30.6 parts by weight of imidazolidine-2-thione were boiled overnight with 54.4 parts by weight of trimethylchlorosilane and 51.5 parts by weight of triethylamine in absolute tetrahydrofurane. The warm suspension was freed of the precipitated triethylamine hydrochloride by filtration, and the filtrate was evaporated and dried in a vacuum desiccator. Melting point: approx. 130°C; Yield: 97%. Calculated: N, 14.4; S, 16.5; Found: N, 13.8; S, 16.9.
References:
US3933795,1976,A
685-91-6
222 suppliers
$38.00/25mL
554-68-7
484 suppliers
$6.00/25g
131933-37-4
0 suppliers
inquiry
96-53-7
314 suppliers
$6.00/10g
![Methanone, 1,1'-[2,3-bis(phenylmethoxy)-1,4-phenylene]bis[1-(2-thioxo-3-thiazolidinyl)-](/CAS/20210305/GIF/492454-84-9.gif)
492454-84-9
0 suppliers
inquiry
554-68-7
484 suppliers
$6.00/25g
4856-97-7
234 suppliers
$6.00/1g
814-49-3
5 suppliers
$41.36/25g
1428649-67-5
0 suppliers
inquiry
554-68-7
484 suppliers
$6.00/25g