ChemicalBook CAS DataBase List Titanous chloride

Titanous chloride synthesis

5synthesis methods

Product Name:Titanous chloride
CAS Number:7705-07-9
Molecular formula:Cl2Ti
Molecular Weight:118.77

Titanium trichloride may be prepared by reducing titanium tetrachloride with hydrogen at 600°C. The tetrachloride may alternatively be reduced with aluminum, zinc, magnesium, tin, or by electrolysis.

Titanium, bis[(1,2,3,4,5,6-η)-methylbenzene]-

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7705-07-9
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Yield:7705-07-9 62%

Reaction Conditions:

in n-heptane;byproducts: CH3C6H5; under purified Ar atm.; soln. of TiCl4 in heptane added to soln. of Ti(η6-MeC6H5)2 in heptane; mixt. stirred for 18 h at room temp.; solid filtered; washed (heptane); dried (vac.); elem. anal.;

References:

Calderazzo, Fausto;Englert, Ulli;Pampaloni, Guido;Volpe, Manuel [Journal of Organometallic Chemistry,2005,vol. 690,# 14,p. 3321 - 3332]

7550-45-0
327 suppliers
$10.00/10g

7705-07-9
117 suppliers
$75.70/250ML

References