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ChemicalBook CAS DataBase List THYMOQUINONE
490-91-5

THYMOQUINONE synthesis

6synthesis methods
-

Yield:490-91-5 93%

Reaction Conditions:

with [N,N'-bis(salicylidene)ethane-1,2-diaminato]cobalt(II);oxygen in N,N-dimethyl-formamide

Steps:

5.2. para-Benzoquinone synthesis23
General procedure: The phenols were oxidized with O2 in DMF, in the presence of Co(salen)2 according to our published procedures: the para-benzoquinone products are normally purified by sublimation

References:

Uliana, Marciana P.;Servilha, Bruno M.;Alexopoulos, Olga;De Oliveira, Kleber T.;Tormena, Cláudio F.;Ferreira, Marco A.B.;Brocksom, Timothy J. [Tetrahedron,2014,vol. 70,# 39,p. 6963 - 6973]

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