TERT-BUTYLSULFAMOYL CHLORIDE synthesis
- Product Name:TERT-BUTYLSULFAMOYL CHLORIDE
- CAS Number:33581-95-2
- Molecular formula:C4H10ClNO2S
- Molecular Weight:171.65
75-64-9
443 suppliers
$10.00/10g
33581-95-2
18 suppliers
$45.00/25mg
Yield:33581-95-2 93%
Reaction Conditions:
with sulfuryl dichloride in acetonitrile; for 24 h;Reflux;
Steps:
44.1
Step 1 : ert-Butylsulfamoyl chloride (P44a) To a solution of fert-butylamine (21.9 g, 0.30 mol) in ACN (150 mL) was added S02CI2 (80 mL) dropwise and the reaction mixture was heated to reflux for 24 h, cooled and concentrated to afford the crude product P44a as a yellow oil (48.0 g, 93%).
References:
WO2012/139775,2012,A1 Location in patent:Page/Page column 68-69
1189-71-5
358 suppliers
$18.00/5g
75-65-0
772 suppliers
$10.00/10ml
33581-95-2
18 suppliers
$45.00/25mg
75-65-0
772 suppliers
$10.00/10ml
33581-95-2
18 suppliers
$45.00/25mg
10017-37-5
59 suppliers
$14.00/1g
33581-95-2
18 suppliers
$45.00/25mg