tert-Butyl thiazolidine-3-carboxylate synthesis
- Product Name:tert-Butyl thiazolidine-3-carboxylate
- CAS Number:148312-55-4
- Molecular formula:C8H15NO2S
- Molecular Weight:189.28
173604-22-3
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148312-55-4
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: LiEt3BH / tetrahydrofuran / 2 h / -78 °C
2: 63 percent / DMAP / pyridine / 1 h / Ambient temperature
3: 83 percent / triethylsilane, trimethylsilyl trifluoromethanesulfonate / 10 h / Ambient temperature
References:
Rassu;Rassu, Gloria;Zanardi;Zanardi, Franca;Cornia;Cornia, Mara;Casiraghi;Casiraghi, Giovanni [Nucleosides and Nucleotides,1996,vol. 15,# 5,p. 1113 - 1120]