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ChemicalBook CAS DataBase List Sinitrodil
143248-63-9

Sinitrodil synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) p-toluenesulfonic acid, 2.) 3N aq. HCl / 1.) toluene, 2 h, reflux, 2.) THF, 24 h, reflux
2: 95 percent / thionyl chloride / CHCl3 / 3 h / Heating
3: 88 percent / silver nitrate / acetonitrile / 2 h / Heating

References:

Benedini, Francesca;Bertolini, Giorgio;Cereda, Roberta;Dona, Giancarlo;Gromo, Gianni;et al. [Journal of Medicinal Chemistry,1995,vol. 38,# 1,p. 130 - 136]

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