(R)-(+)-1-AMINO-2-(METHOXYMETHYL)PYRROLIDINE synthesis
- Product Name:(R)-(+)-1-AMINO-2-(METHOXYMETHYL)PYRROLIDINE
- CAS Number:72748-99-3
- Molecular formula:C6H14N2O
- Molecular Weight:130.19
68832-13-3
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Yield:-
Steps:
Multi-step reaction with 5 steps
1.1: 0.83 h / 0 °C
2.1: sodium hydride / tetrahydrofuran / -60 - -50 °C / Inert atmosphere
3.1: potassium hydroxide / water / 20 °C / Inert atmosphere
3.2: Cooling with ice
4.1: potassium hydroxide / water / 12 h / 15 - 20 °C / pH 2.8 - 3.2
5.1: potassium hydroxide; potassium hypochlorite / water / -5 - 40 °C
References:
Enders, Dieter;Fey, Peter;Kipphardt, Helmut [Organic Syntheses,1987,vol. 65,p. 173 - 173]
121817-72-9
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344-25-2
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72748-98-2
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72748-99-3
102 suppliers
$55.00/250mg