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ChemicalBook CAS DataBase List (+)-PINANEBORANE
90084-43-8

(+)-PINANEBORANE synthesis

2synthesis methods
-

Yield:-

Reaction Conditions:

with dimethylsulfide borane complex in 1,4-dioxane;

Steps:

26

[00277] A stock solution of the borane (1S,2S,6R,8S)-2,9,9-trimethyl-3,5-dioxa-4-boratricyclo[6.1.1.02,6]decane was synthesised from the diol (1.96 g; 11.5 mmol) and 1.1 ml of BH3?e2 solution (11 mmol) in 20 ml dioxane.

References:

US6680401,2004,B1 Location in patent:Page column 43

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