perylene-3,4,9,10-tetracarboxylic acid synthesis

8synthesis methods

Product Name:perylene-3,4,9,10-tetracarboxylic acid
CAS Number:81-32-3
Molecular formula:C24H12O8
Molecular Weight:428.35

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 59 percent / Cl₂, 3percent oleum / 9 h / 70 - 75 °C
2: 91 percent / KOH / ethane-1,2-diol / 4 h / 155 - 160 °C

References:

Rogovik, V. I.;Gutnik, L. F. [Journal of Organic Chemistry USSR (English Translation),1988,vol. 24,# 3,p. 569 - 573][Zhurnal Organicheskoi Khimii,1988,vol. 24,# 3,p. 635 - 639]

128-69-8 Synthesis

3,4,9,10-Perylenetetracarboxylic dianhydride

128-69-8
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References

3,4,9,10-Perylenetetracarboxylic acid, 1,6,7,12-tetrachloro-

118153-98-3
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81-32-3
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References

3,4,9,10-Perylenetetracarboxylic acid, 1,7-dibromo-

107905-43-1
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81-32-3
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References

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81-32-3
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References

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