Perfluoroheptanoic acid synthesis
- Product Name:Perfluoroheptanoic acid
- CAS Number:375-85-9
- Molecular formula:C7HF13O2
- Molecular Weight:364.06
375-84-8
41 suppliers
$41.00/5g
375-85-9
191 suppliers
$5.00/100mg
Yield:375-85-9 89 g
Reaction Conditions:
with water at 50; for 3 h;Temperature;
Steps:
3.2 Example 3
(2) The resulting product was added to the fluorination reactor at a temperature of 50 ,From the bottom of the reactor 200ml / min speed of 25% of the fluorine gas. Continued ventilation 25 hours,Sampling test, the raw material completely reacted. Receipt of 112 grams,The yield was 96%, the product of fluorination was warmed to 50 ° C, 9 g of deionized water was added,Continue stirring for 3 hours. Negative pressure distillation, to give the product 89 grams, purity 96.2%. The overall yield of 75.6%.
References:
Jinan Qifu New Materials Co., Ltd.;Zhang Liting CN106831388, 2017, A Location in patent:Paragraph 00114; 0015; 0016
52447-22-0
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$45.00/1 g
375-85-9
191 suppliers
$5.00/100mg
559-14-8
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$40.00/500mg
375-85-9
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$5.00/100mg
355-43-1
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$10.00/10 g
124-38-9
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$175.00/23402
375-85-9
191 suppliers
$5.00/100mg
20109-59-5
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375-85-9
191 suppliers
$5.00/100mg