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ChemicalBook CAS DataBase List O-Benzyl-D-serine
10433-52-0

O-Benzyl-D-serine synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 1.) butyllithium / 1.) THF, hexane, - 70 deg C, 2.) - 70 deg C, 12 h
2: 1.) 0.1 N aq. HCl, 2.) 25percent aq. NH3 / 1.) room temp., 12 h
3: 2N aq. HCl / 1 h / Heating
4: methyloxirane / ethanol / 0.25 h / Heating

References:

Nozulak, Joachim;Schoellkopf, Ulrich [Synthesis,1982,# 10,p. 866 - 868]

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