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ChemicalBook CAS DataBase List Nitrosylsulfuric acid
7782-78-7

Nitrosylsulfuric acid synthesis

5synthesis methods
-

Yield:-

Reaction Conditions:

in acetic acidInert atmosphere;

Steps:


Nitrosyl hydrogensulfate was synthesized by bubbling dried SO2 into fuming nitric acid (100 mL, 2.4 mol) for several hours, followed by filtration and rinsing with glacial acetic acid and tetrachloromethane under argon.

References:

Lippold, Marcus;Boehme, Uwe;Gondek, Christoph;Kronstein, Martin;Patzig-Klein, Sebastian;Weser, Martin;Kroke, Edwin [European Journal of Inorganic Chemistry,2012,# 34,p. 5714 - 5721]

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