ChemicalBook CAS DataBase List NAPHTHO[1,2,3,4-GHI]PERYLENE

NAPHTHO[1,2,3,4-GHI]PERYLENE synthesis

8synthesis methods

Product Name:NAPHTHO[1,2,3,4-GHI]PERYLENE
CAS Number:190-84-1
Molecular formula:C26H14
Molecular Weight:326.39

198-55-0
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118-92-3
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190-84-1
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Yield:190-84-1 77%

Reaction Conditions:

Stage #1: anthranilic acidwith para-dodecylbenzenesulfonic acid;isopentyl nitrite in ethyl acetate at 25; for 1 h;Diels-Alder Cycloaddition;
Stage #2: PERYLENEwith potassium fluoride;18-crown-6 ether in toluene at 100; for 2 h;Diels-Alder Cycloaddition;Solvent;

References:

Pavlyuk;Gundala;Kovalev;Kopchuk;Krinochkin;Budeev;Zyryanov;Venkatapuram;Rusinov;Chupakhin [Russian Journal of Organic Chemistry,2019,vol. 55,# 3,p. 409 - 411][Zh. Org. Khim.,2019,vol. 55,# 3,p. 477 - 480,4]

198-55-0
242 suppliers
$6.00/1g

88284-48-4 Synthesis