ChemicalBook CAS DataBase List N N-DI-N-HEXYLANILINE 97

N N-DI-N-HEXYLANILINE 97 synthesis

14synthesis methods

Product Name:N N-DI-N-HEXYLANILINE 97
CAS Number:4430-09-5
Molecular formula:C18H31N
Molecular Weight:261.45

3839-35-8
57 suppliers
$50.00/5g

62-53-3 Synthesis

62-53-3
660 suppliers
$10.00/1g

4430-09-5
19 suppliers
$842.13/5G

Yield:4430-09-5 93%

Reaction Conditions:

with tetrabutylammomium bromide;sodium hydroxide at 100; for 8 h;

Steps:

5

Taking paratoluene sulfonic acid hexyl 2.56 g (0.01 μM), normal temperature by the addition of 0.33 g (0.0036 μM) aniline, adding 0.05 g ammonium bromide [...] transfer catalyst, heating up to 100 °C dropwise 25% sodium hydroxide solution of 1.6 g (0.01 μM), maintaining the temperature reaction 8 h after, to room temperature, extracted with ethyl acetate, dried and filtered, rotary evaporation, can be dark purple viscous liquid, by silica gel column to obtain a pale yellow liquid 0.87 g, N, N - dihexylacrylamide aniline of the yield is 93%.

References:

CN109942436,2019,A Location in patent:Paragraph 0076; 0078