ChemicalBook CAS DataBase List N-HEXYLTRIMETHOXYSILANE

N-HEXYLTRIMETHOXYSILANE synthesis

3synthesis methods

Product Name:N-HEXYLTRIMETHOXYSILANE
CAS Number:3069-19-0
Molecular formula:C9H22O3Si
Molecular Weight:206.35

592-41-6 Synthesis

592-41-6
261 suppliers
$10.00/5g

2487-90-3 Synthesis

2487-90-3
290 suppliers
$130.00/5g

3069-19-0
147 suppliers
$7.00/5g

Yield:3069-19-0 100%

Reaction Conditions:

at 90; for 5 h;Inert atmosphere;

Steps:

17 Example 17

In a 500-ml three-necked flask, hexene (1.25 mol) was added, and Catalyst 1 (1.25 mmol) prepared in Example 1 was slowly heated to 90°C under nitrogen protection.While stirring, trimethoxyhydrosilane (1.5 mol) was added dropwise via a dropping funnel. The dropwise addition time was 0.5 hours. The reaction temperature was maintained and the reaction was continued for 5 hours.After cooling to room temperature, the corresponding fraction was collected by distillation under reduced pressure, and the conversion of hexene was determined by GC-MS to be 89.0%.The yield of the β adduct 1-trimethoxysilylhexane was 100%.

References:

CN107857776,2018,A Location in patent:Paragraph 0060; 0061