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52721-77-4

N-FORMYL-4-IODO-L-PHENYLALANINE synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: peracetic acid; sulfuric acid; iodine; acetic acid / 2 - 4 h / 55 °C
1.2: 2 h / 50 - 55 °C
1.3: 1 h / 10 - 15 °C
2.1: sodium hydroxide / methanol; water / 4 h / 22 °C
2.2: 1 - 2 h / 31 °C / pH 1

References:

WO2003/104200,2003,A1

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