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458550-44-2

N-(4-BROMOPHENYL-N-(4-CARBETHOXYPHENYL)AMINE synthesis

7synthesis methods
-

Yield:458550-44-2 73%

Reaction Conditions:

Stage #1: 4-iodobenzoic acid ethyl esterwith isopropylmagnesium chloride in tetrahydrofuran at -20; for 0.5 h;
Stage #2: para-nitrophenyl bromide in tetrahydrofuran at -20; for 2 h;
Stage #3: with sodium tetrahydroborate;iron(II) chloride in tetrahydrofuran;ethanol at 20; for 2 h;Further stages.;

References:

Sapountzis, Ioannis;Knochel, Paul [Journal of the American Chemical Society,2002,vol. 124,# 32,p. 9390 - 9391]

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