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ChemicalBook CAS DataBase List N-(11-Bromoundecyl)carbamic acid tert-butyl ester
463930-53-2

N-(11-Bromoundecyl)carbamic acid tert-butyl ester synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 53 percent / LiAlH4 / tetrahydrofuran / 6 h / 67 °C
2: 89 percent / Et3N / CH2Cl2 / 10 h / 0 - 23 °C
3: 74 percent / N-bromosuccinimide; Ph3P / benzene / 12 h / 23 °C

References:

Belser, Thomas;Stoehr, Meike;Pfaltz, Andreas [Journal of the American Chemical Society,2005,vol. 127,# 24,p. 8720 - 8731]