MONOCROTALINE synthesis
- Product Name:MONOCROTALINE
- CAS Number:315-22-0
- Molecular formula:C16H23NO6
- Molecular Weight:325.36
![1,3-Dioxolane-4-acetic acid, α,4,5-trimethyl-5-[[2-(trimethylsilyl)ethoxy]carbonyl]-, 2,3,5,7a-tetrahydro-7-(hydroxymethyl)-1H-pyrrolizin-1-yl ester, [1α[R*(4R*,5R*)],7aβ]- (9CI)](/CAS/20210305/GIF/109391-29-9.gif)
109391-29-9
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315-22-0
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: Et3N / CH2Cl2
2: 71 percent / Bu4N(1+)F(1-)*3H2O / acetonitrile / 34 °C
3: 75 percent / 38percent HCl / ethane-1,2-diol / 2 h / 110 °C
References:
Vedejs;Ahmad;Larsen;Westwood [Journal of Organic Chemistry,1987,vol. 52,# 17,p. 3937 - 3938]
35337-98-5
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315-22-0
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![1,3-Dioxolane-4-acetic acid, α,4,5-trimethyl-5-[[2-(trimethylsilyl)ethoxy]carbonyl]-, 7-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-2,3,5,7a-tetrahydro-1H-pyrrolizin-1-yl ester, [4α[αR*(1R*,7aR*)],5α]- (9CI)](/CAS/20210305/GIF/109432-25-9.gif)
109432-25-9
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315-22-0
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![1H-Pyrrolizin-1-ol, 7-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-2,3,5,7a-tetrahydro-, lithium salt (1:1), (1R,7aR)-rel-](/CAS/20211123/GIF/89710-47-4.gif)
89710-47-4
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315-22-0
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121719-94-6
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315-22-0
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$35.00/10mg