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ChemicalBook CAS DataBase List METHYL (S)-(+)-3-HYDROXY-2-METHYLPROPIONATE
80657-57-4

METHYL (S)-(+)-3-HYDROXY-2-METHYLPROPIONATE synthesis

5synthesis methods
-

Yield:80657-57-4 87%

Reaction Conditions:

with diisopropyl{1-[(S)-3,5-dioxa-4-phospha-cyclohepta(2,1-a;3,4-a')dinaphthalen-4-yl]-3-methyl-2-indolyl}phosphine;bis(norbornadiene)rhodium(l)tetrafluoroborate;hydrogen in dichloromethane at -40; under 15001.5 Torr; for 15 h;Reactivity;Inert atmosphere;optical yield given as %ee;enantioselective reaction;Pressure;Temperature;Concentration;

References:

Wassenaar, Jeroen;Kuil, Mark;Reek, Joost N. H. [Advanced Synthesis and Catalysis,2008,vol. 350,# 10,p. 1610 - 1614] Location in patent:supporting information; experimental part

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