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ChemicalBook CAS DataBase List Methyl beta-D-ribofuranoside
7473-45-2

Methyl beta-D-ribofuranoside synthesis

10synthesis methods
-

Yield:7473-45-2 55 mg

Reaction Conditions:

Stage #1: methanolwith acetyl chloride at 0 - 5; for 0.333333 h;
Stage #2: β-D-ribofuranose at 20; for 24 h;Time;

Steps:

1 (Example 1)

Add 300 ml of anhydrous methanol to a 500 ml single-mouth bottle, cool to 0-5°C in an ice bath, add 5.2 g (20 mol%) of acetyl chloride slowly, incubate and stir for 20 minutes, add 50 g of D-ribose, and raise to room temperature. After 24 hours, the solvent was concentrated to give 55 g of a white solid product, methyl-[beta]-D-nucleoside.

References:

CN106565805,2017,A Location in patent:Paragraph 0027; 0028; 0036; 0037

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