METHYL 4-PYRROLIDIN-1-YLBENZOATE synthesis
- Product Name:METHYL 4-PYRROLIDIN-1-YLBENZOATE
- CAS Number:129414-26-2
- Molecular formula:C12H15NO2
- Molecular Weight:205.25
67-56-1
776 suppliers
$9.00/25ml
22090-27-3
90 suppliers
$10.00/500mg
129414-26-2
56 suppliers
$68.00/1g
Yield:129414-26-2 95%
Reaction Conditions:
with thionyl chloride for 5 h;Reagent/catalyst;
Steps:
Esterification of p-Aminobenzoic Acida) With Thionyl Chloride and Methanol24
General procedure: To a solution of the benzoic acid derivative (10 mmol) in anhydrous methanol (35 mL)was added dropwise thionyl chloride (1.1 mL, 15 mmol) under vigorous stirring (stirbar). After 5 h, about 25 mL of the methanol was distilled off and the residue was pouredonto 50 mL of ice water. Then saturated aqueous sodium bicarbonate was added withstirring until the evolution of carbon dioxide ceased. The resulting precipitate wascollected and recrystallized from methanol.
References:
Pietrzak, Marek;J?drzejewska, Beata;M?drzejewska, Dorota;Bajorek, Agnieszka [Organic Preparations and Procedures International,2017,vol. 49,# 1,p. 45 - 52]
123-75-1
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$10.00/5g
619-44-3
313 suppliers
$6.00/10g
129414-26-2
56 suppliers
$68.00/1g
15097-49-1
50 suppliers
$167.00/25g
403-33-8
328 suppliers
$13.43/1gm:
129414-26-2
56 suppliers
$68.00/1g
123-75-1
576 suppliers
$10.00/5g
619-42-1
368 suppliers
$7.00/10g
129414-26-2
56 suppliers
$68.00/1g
110-63-4
711 suppliers
$24.80/250g
619-45-4
395 suppliers
$6.00/1g
129414-26-2
56 suppliers
$68.00/1g