Methyl 4-ethoxybenzoate synthesis
- Product Name:Methyl 4-ethoxybenzoate
- CAS Number:23676-08-6
- Molecular formula:C10H12O3
- Molecular Weight:180.2
Yield:23676-08-6 99.64%
Reaction Conditions:
with potassium carbonate in butanone at 78 - 80; for 2 h;
Steps:
Methyl-4-ethoxy benzoate (3)
To the stirred solution of methyl paraben (0.100 Kg, 0.657 mol) was treated with diethyl sulphate (0.152 Kg, 0.98 mol) in the presence of potassium carbonate (0.181 Kg, 1.31 mol) in 2-butanone (700 mL). Followed the procedure as mentioned in compound (2) and isolated the product (3). Yield: 0.118 Kg, 99.64 %.
References:
Periyasamy, Senthil;Subbiah, Selvaraj [Asian Journal of Chemistry,2018,vol. 30,# 1,p. 85 - 88]
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