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40216-71-5

Methyl 2-(benzylideneamino)propanoate synthesis

3synthesis methods
-

Yield:40216-71-5 98%

Reaction Conditions:

Stage #1: methyl 2-aminopropanoate monohydrochloridewith magnesium sulfate in dichloromethane at 20; for 0.333333 h;Inert atmosphere;
Stage #2: benzaldehydewith triethylamine in dichloromethane at 20;Inert atmosphere;

References:

Griffiths-Jones (née Haskins), Charlotte M.;Knight, David W. [Tetrahedron,2010,vol. 66,# 23,p. 4150 - 4166] Location in patent:experimental part